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  1. Asked: July 24, 2020In: Thermocouples

    What is a workload thermocouple and what does it look like inside?

    VacuumFurnaces.com Answers
    Added an answer on October 3, 2023 at 12:40 pm
    This answer was edited.

    A thermocouple is a sensor that measures temperature. It consists of two different types of metals, joined together at one end. When the junction of the two metals is heated or cooled, a voltage is created that can be correlated back to the temperature. A thermocouple is a simple, robust and cost-efRead more

    A thermocouple is a sensor that measures temperature. It consists of two different types of metals, joined together at one end. When the junction of the two metals is heated or cooled, a voltage is created that can be correlated back to the temperature. A thermocouple is a simple, robust and cost-effective temperature sensor used in a wide range of temperature measurement processes.

    READ MORE: https://www.omega.com/en-us/resources/thermocouple-hub

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  2. Asked: March 1, 2021In: Cryogenic Pumps

    Why must the cryogenic medium used to cool the cold trap between the gas manifold and the mechanical pump be liquid nitrogen?

    VacuumFurnaces.com Answers
    Added an answer on March 31, 2023 at 6:16 pm
    This answer was edited.

    Liquid nitrogen cold traps prevent products arising during the equipment operation from passing from the chamber into the pump where they could either contaminate the pump or cause the breakdown of the pump fluid. In either case, severe loss of efficiency and poor vacuum levels result. In the examplRead more

    Liquid nitrogen cold traps prevent products arising during the equipment operation from passing from the chamber into the pump where they could either contaminate the pump or cause the breakdown of the pump fluid. In either case, severe loss of efficiency and poor vacuum levels result. In the example shown the diffusion pump was only capable of reaching 4 x 10-3 Torr rather than the typical 1 x 10-5 Torr range achieved with a clean pump. In addition, these types of cold traps prevent backstreaming of the pump.

    SOURCE: Cold Traps / VAC AERO International Inc.

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  3. Asked: March 6, 2021In: Vacuum Pumping System

    What are some common vacuum furnace pumping system failures and their solutions?

    VacuumFurnaces.com Answers
    Added an answer on March 30, 2023 at 4:29 pm
    Home

    For the many vacuum furnaces in use around the world, the vacuum pumping system is a critical component. To get the best value from the vacuum furnace system and to extend its useful life, the regular and careful maintenance of the various vacuum pumps is of utmost importance.  Here are two resourceRead more

    For the many vacuum furnaces in use around the world, the vacuum pumping system is a critical component. To get the best value from the vacuum furnace system and to extend its useful life, the regular and careful maintenance of the various vacuum pumps is of utmost importance. 
    Here are two resources that delve deeply into this question, courtesy of Solar Atmospheres and Bill Jone.
    This PDF published by Solar Atmospheres Inc. and a Youtube Video presented by the legendary founder of Solar Atmospheres, Bill Jones

    SOURCE: Solar Atmospheres Inc. https://solaratm.com/

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  4. Asked: April 13, 2021In: Leak Checking, Testing & Detection

    What are acceptable helium leak rates?

    VacuumFurnaces.com Answers
    Added an answer on March 30, 2023 at 3:49 pm

    The leak-up rate you should be looking for depends primarily on the type of base metals you are trying to braze. As mentioned at the beginning of this article, any air leak into the furnace represents an influx of oxygen into the furnace. Metals vary considerably in their tolerance of oxygen, with nRead more

    The leak-up rate you should be looking for depends primarily on the type of base metals you are trying to braze. As mentioned at the beginning of this article, any air leak into the furnace represents an influx of oxygen into the furnace. Metals vary considerably in their tolerance of oxygen, with nickel and gold being examples of metals that have a large tolerance for the presence of oxygen. That is, they will not oxidize to the point that there is any negative effect on brazing.

    However, other metals, such as chromium, or base metals which contain titanium and/or aluminum in their chemistry, will be highly sensitive to the presence of any oxygen in the furnace. Thus, may I suggest the following as a guideline for vacuum-furnace brazing:

    Tolerable Vacuum Furnace Leak-up Rates:

    • For base metals that contain any titanium or aluminum: less than five (5) microns per hour.
    • For base metals containing chromium (Cr), or manganese (Mn) but no titanium and/or aluminum: less than ten (10) microns per hour.
    • For base metals containing nickel (Ni), gold (Au), etc., but without any Cr or Mn or Ti or Al: less than fifteen (15) microns per hour.>>> READ MORE

    SOURCE: Kay & Assoc. Brazing Consultants

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  5. Asked: July 26, 2021In: Instruments - Calibration

    What is an AMS2750 calibration survey?

    VacuumFurnaces.com Answers
    Added an answer on March 30, 2023 at 3:34 pm

    Our blog post takes a short look at the AMS2750E standard, with a special focus on the requirements set for calibration, calibration accuracy, and test/calibration equipment. The AMS2750E is predominantly designed for heat treatment in the aerospace industry. Heat treatment is an essential process fRead more

    Our blog post takes a short look at the AMS2750E standard, with a special focus on the requirements set for calibration, calibration accuracy, and test/calibration equipment. The AMS2750E is predominantly designed for heat treatment in the aerospace industry. Heat treatment is an essential process for many critical parts of an airplane, so it is understandable that there are tight regulations and audit processes set. While the results and success of some other industrial processes can be relatively easily measured after the process, this is not the case in a heat treatment process. Therefore, very tight control and documentation of the heat treatment process are essential to ensure the quality of the end products.>>>READ MORE

    Source: Beamex Blog for Calibration Professionals

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  6. Asked: March 2, 2023In: Vacuum Furnaces, Vacuum Pump Maintenance, Vacuum Pump Performance Checks, Vacuum Pumps

    HOW CAN I CELANİNG CONTAMİNATİON OF VACUUM FURNACES?

    VacuumFurnaces.com Answers
    Added an answer on March 30, 2023 at 3:27 pm

    "When operating vacuum furnaces, situations may arise in which the hot zone and/or cold walls may become contaminated (Fig. Nos. 1 – 2). This can occur from a variety of sources: air leaks, outgassing from residues left on the parts as a result of the manufacturing or cleaning processes, vaporizatioRead more

    “When operating vacuum furnaces, situations may arise in which the hot zone and/or cold walls may become contaminated (Fig. Nos. 1 – 2). This can occur from a variety of sources: air leaks, outgassing from residues left on the parts as a result of the manufacturing or cleaning processes, vaporization of sensitive materials (e.g., chromium-bearing materials), process-induced contaminations such as carbon in the form of soot or tar, fluxes from brazing pastes, excess braze alloy as well as many other sources. Often times the work being processed is also affected (Fig. 3). The question becomes, how do we attempt to clean up our contaminated vacuum furnaces? >>>Read More

    Source: VAC AERO International

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  7. Asked: February 25, 2021In: Diffusion Pumps

    How does a diffusion pump work?

    Ryan
    Added an answer on March 13, 2023 at 8:24 pm

      I have provided a diagram above to aid in this answer. The diffusion pump is a very common mechanism for creating a high vacuum. Generally, the pump contains three cone-shaped pressure jets stacked vertically. There is pump oil at the bottom that is heated until it reaches a gaseous state. InRead more

     

    I have provided a diagram above to aid in this answer. The diffusion pump is a very common mechanism for creating a high vacuum. Generally, the pump contains three cone-shaped pressure jets stacked vertically. There is pump oil at the bottom that is heated until it reaches a gaseous state. In the gaseous state, the oil will travel upward and exit through pressure jets in a downward direction. As the vapor travels towards the walls, it will trap air molecules that enter the pump through diffusion. With the cooling coils on the walls, the vapor will immediately condense, releasing the trapped air molecule at a lower position. The oil will travel back to the heater where the process will continue, and the air molecule will be removed via the backing pump and thus creating the high vacuum.

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  8. Asked: January 22, 2023In: Control System – Testing

    Number of SAT Thermocouples Required

    Raf Walczak
    Added an answer on March 3, 2023 at 7:16 pm

    According to paragraph 3.4.1.2. of AMS2750G: "The SAT shall be performed on all control and recording systems required by the applicable instrumentation type, as well as any additional recording systems used for parts and raw material acceptance in each control zone of each piece of thermal processiRead more

    According to paragraph 3.4.1.2. of AMS2750G:
    “The SAT shall be performed on all control and recording systems required by the applicable instrumentation type, as well as any additional recording systems used for parts and raw material acceptance in each control zone of each piece of thermal processing equipment used for production heat treatments.”

    That means you should perform SAT on all control temperatures as well as any other temperature measurement system which are required by instrumentation type. For example Load thermocouples for instrumentation type A and B.
    SAT is not required for overtemp systems (if overtemp protection  is the only function of that system).

    Each of those ‘systems’ (Thermocouple, TC wires, feedthroughs, and measuring/recording instrument) should be within SAT tolerance (which is 2F for class 1 equipment) to their SAT sensor.

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  9. Asked: March 2, 2023In: Heating Chamber - Hot Zone

    Burn in cycle for new hot zone

    Raf Walczak
    Added an answer on March 3, 2023 at 6:39 pm

    Furnace burn out (a.k.a. thermal cleaning) cycles are important part of vacuum furnace maintenance. It is meant to reduce and outgas contaminants inside the heating zone and within the insulation. For new hot zone it is more related to drying, conditioning and outgassing the remaining resin from insRead more

    Furnace burn out (a.k.a. thermal cleaning) cycles are important part of vacuum furnace maintenance. It is meant to reduce and outgas contaminants inside the heating zone and within the insulation.

    For new hot zone it is more related to drying, conditioning and outgassing the remaining resin from insulation manufacturing processes. Every new furnace should be burned out at it’s nominal temperature and I’d say this rule should also apply to any hot zone replacement. Your hot zone supplier should be able to tell you the nominal temperature of the hot zone.

    Duration of burnout should be at least 2 hours at the temperature, however you may keep it longer if you see continuous improvement of furnace vacuum level.
    Slow cooling is recommended after burnout.

    IMPORTANT: The burn-out cycle is always performed with empty furnace. any tooling / fixturing and other equipment must be removed otherwise serious damage of furnace and tooling may occur.
    For your own safety you should follow the OEM manuals.

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  10. Asked: March 1, 2021In: Vacuum Technology

    What does it mean when a unit of measurement is raised to a negative power?

    Thomas
    Added an answer on June 20, 2022 at 3:30 am

    When a number is raised to a negative power, in fraction form it would be described as one over that number and its exponent (positive). See below: This is also how negative powers work when applied to units. The well known constituent units of the Newton (Force) kg*m/(s^2) could also be written asRead more

    When a number is raised to a negative power, in fraction form it would be described as one over that number and its exponent (positive). See below:

    This is also how negative powers work when applied to units. The well known constituent units of the Newton (Force) kg*m/(s^2) could also be written as kg*m*s^-2, and so on. The negative exponent would represent the ‘per’, e.g. kilograms meters ‘per’ second squared.

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  11. Asked: March 1, 2021In: Quench Cooling System

    What are the benefits of argon gas quench?

    Thomas
    Added an answer on June 20, 2022 at 3:17 am

    ARGON is an inert gas used in gas quenching, thus it has certain inherent advantages over liquid quenching media. Namely: Gas quenched materials have cleaner surfaces and experience less oxidation [1] Gas quenching allows for less deformities and more uniform cooling [1] Gas quenching is safer [2] GRead more

    ARGON is an inert gas used in gas quenching, thus it has certain inherent advantages over liquid quenching media. Namely:

    1. Gas quenched materials have cleaner surfaces and experience less oxidation [1]
    2. Gas quenching allows for less deformities and more uniform cooling [1]
    3. Gas quenching is safer [2]
    4. Gas quenching poses less risk to the environment (particularly when compared to oil quenching) [2]

    There are other gas quenching media, however. One (popular) gas is nitrogen. Nitrogen is more often used because it is cheaper with a faster cooling rate [3].

    However, nitrogen can decarburize [3] or nitride [4] sensitive steels, whereas argon does not. Furthermore, when compared directly to nitrogen over a handful of samples, in most cases, argon quenched steel had slightly or significantly better mechanical properties [3].


    References

    [1] https://www.generon.com/nitrogen-quenching-system/

    [2] https://www.lindeus.com/industries/manufacturing-and-materials-processing/gas-quenching-and-inerting

    [3] https://www.industrialheating.com/articles/93972-comparing-argon-and-nitrogen-cooling-in-vacuum-furnaces

    [4]https://www.boconline.co.uk/en/images/Principles%20of%20Quenching%20and%20Cooling_tcm410-114391.pdf

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  12. Asked: April 7, 2021In: Leak Checking, Testing & Detection

    Are vacuum furnace leak rates linear?

    rcauthon CWI
    Added an answer on January 25, 2022 at 8:41 pm

    Leak rates are not typically linear in nature.

    Leak rates are not typically linear in nature.

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  13. Asked: July 30, 2020In: Vacuum Pumps

    What is the working principle of a momentum transfer pump?

    Anonymous
    Added an answer on September 14, 2021 at 3:37 pm

    A transfer pump is used to transfer various gases and liquids from one position to another position. This type of pump moves fuel from a container to a nozzle or from one tank to another so that it can be distributed to automobiles. The pumps can also move fuel from one vehicle to another or take ouRead more

    A transfer pump is used to transfer various gases and liquids from one position to another position. This type of pump moves fuel from a container to a nozzle or from one tank to another so that it can be distributed to automobiles. The pumps can also move fuel from one vehicle to another or take out fuel from an automobile and return it to a storage vessel. Diesel transfer pump uses to fuel all types of diesel automobiles, including plant equipment, truck vehicles, cars, coaches, trucks, and buses, etc. Diesel transfer pump presents in the fueling system that allows fuel to move from one location to the desired location. These pumps also use in various industries and adaptable applications.

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  14. Asked: July 24, 2020In: Diffusion Pumps

    What are the steps for cleaning diffusion pump cooling lines?

    Kevin Tracy
    Added an answer on September 14, 2021 at 3:37 pm

    Disconnect the lines and add additional temporary plumbing to flush the system with a pump and 2 buckets. Use a solution of CLR and water in one bucket and flush through the lines to the other bucket. Preferably, flush backwards through the system to break things up first, then flush through in theRead more

    Disconnect the lines and add additional temporary plumbing to flush the system with a pump and 2 buckets. Use a solution of CLR and water in one bucket and flush through the lines to the other bucket. Preferably, flush backwards through the system to break things up first, then flush through in the normal direction. Flush with plain water before reconnecting the system. If this does not work, repeat the process with a solution of muriatic acid.

    See manufacturer recommendation for chemical mixtures and MSDS for safety.

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  15. Asked: February 6, 2021In: Temperature Uniformity Survey (TUS)

    When should we perform Temperature Uniformity Surveys (TUS)?

    viczac
    Added an answer on August 10, 2021 at 6:15 pm

    In general, we can say that there are two circumstances: 1) According to the frequency specified by the applicable standard (AMS2750, CQI-9, API) 2) When a modification is made to the equipment. Here it is important to be clear about the word "modification". In general terms, a modification is an alRead more

    In general, we can say that there are two circumstances:

    1) According to the frequency specified by the applicable standard (AMS2750, CQI-9, API)

    2) When a modification is made to the equipment.

    Here it is important to be clear about the word “modification”. In general terms, a modification is an alteration or adjustment that could affect the thermal characteristics of the equipment.

    Both #AMS2570 and #CQI9 provide very clear guidance on what is a modification and what is not. Some examples of equipment modification:

    • Change in the qualified operating temperature or work zone.
    • Change in burner/heating element type or location.
    • Changes to airflow.
    • Change of refractory thickness or new refractory with different thermal properties.
    • Change of control sensor location.
    • Change of combustion settings.
    • Adjustment of control instrument tuning constants (PID)

    If you want to learn more about these standards, you can follow the blog of Global Thermal Solutions LLC to find useful articles related to #heattreatment management.

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